N-(2-allyl-4-ethoxy-2H-indazol-5-yl)-4-methylbenzenesulfonamide

Hakima Chicha, El Mostapha Rakib, Latifa Bouissane, Maurizio Viale, Mohamed Saadi, Lahcen El Ammari

Research output: Contribution to journal › Article

Abstract

The indazole ring system of the title compound, C19H 21N3O3S, is almost planar (r.m.s. deviation = 0.0192Å) and forms dihedral angles of 77.99(15) and 83.9(3)° with the benzene ring and allyl group, respectively. In the crystal, centrosymmetrically related molecules are connected by pairs of N - H⋯O hydrogen bonds into dimers, which are further linked by C - H⋯O hydrogen bonds, forming columns parallel to the b axis.

Original languageEnglish
JournalActa Crystallographica Section E: Structure Reports Online
Volume70
Issue number5
DOIs
Publication statusPublished - 2014

Fingerprint

Hydrogen bonds
Indazoles
hydrogen bonds
rings
Dihedral angle
Benzene
Dimers
dihedral angle
benzene
dimers
deviation
Crystals
Molecules
crystals
molecules
4-toluenesulfonamide

Keywords

  • data-to-parameter ratio = 17.3
  • mean σ(C-C) = 0.004 A°
  • R factor = 0.046
  • single-crystal X-ray study
  • T = 296 K
  • wR factor = 0.134

ASJC Scopus subject areas

  • Condensed Matter Physics
  • Materials Science(all)
  • Chemistry(all)

Cite this

N-(2-allyl-4-ethoxy-2H-indazol-5-yl)-4-methylbenzenesulfonamide. / Chicha, Hakima; Rakib, El Mostapha; Bouissane, Latifa; Viale, Maurizio; Saadi, Mohamed; El Ammari, Lahcen.

In: Acta Crystallographica Section E: Structure Reports Online, Vol. 70, No. 5, 2014.

Research output: Contribution to journal › Article

Chicha, H, Rakib, EM, Bouissane, L, Viale, M, Saadi, M & El Ammari, L 2014, 'N-(2-allyl-4-ethoxy-2H-indazol-5-yl)-4-methylbenzenesulfonamide', Acta Crystallographica Section E: Structure Reports Online, vol. 70, no. 5. https://doi.org/10.1107/S1600536814009283
Chicha H, Rakib EM, Bouissane L, Viale M, Saadi M, El Ammari L. N-(2-allyl-4-ethoxy-2H-indazol-5-yl)-4-methylbenzenesulfonamide. Acta Crystallographica Section E: Structure Reports Online. 2014;70(5). https://doi.org/10.1107/S1600536814009283
Chicha, Hakima ; Rakib, El Mostapha ; Bouissane, Latifa ; Viale, Maurizio ; Saadi, Mohamed ; El Ammari, Lahcen. / N-(2-allyl-4-ethoxy-2H-indazol-5-yl)-4-methylbenzenesulfonamide. In: Acta Crystallographica Section E: Structure Reports Online. 2014 ; Vol. 70, No. 5.
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AU - Chicha, Hakima

AU - Rakib, El Mostapha

AU - Bouissane, Latifa

AU - Viale, Maurizio

AU - Saadi, Mohamed

AU - El Ammari, Lahcen

PY - 2014

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N2 - The indazole ring system of the title compound, C19H 21N3O3S, is almost planar (r.m.s. deviation = 0.0192Å) and forms dihedral angles of 77.99(15) and 83.9(3)° with the benzene ring and allyl group, respectively. In the crystal, centrosymmetrically related molecules are connected by pairs of N - H⋯O hydrogen bonds into dimers, which are further linked by C - H⋯O hydrogen bonds, forming columns parallel to the b axis.

AB - The indazole ring system of the title compound, C19H 21N3O3S, is almost planar (r.m.s. deviation = 0.0192Å) and forms dihedral angles of 77.99(15) and 83.9(3)° with the benzene ring and allyl group, respectively. In the crystal, centrosymmetrically related molecules are connected by pairs of N - H⋯O hydrogen bonds into dimers, which are further linked by C - H⋯O hydrogen bonds, forming columns parallel to the b axis.

KW - data-to-parameter ratio = 17.3

KW - mean σ(C-C) = 0.004 A°

KW - R factor = 0.046

KW - single-crystal X-ray study

KW - T = 296 K

KW - wR factor = 0.134

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